dc.creator | Przybilla, Thomas | es |
dc.creator | Zubiri, Benjamin | es |
dc.creator | Beltrán, Ana M. | es |
dc.creator | Butz, Benjamin | es |
dc.creator | Machoke, Albert Gonche | es |
dc.creator | Inayat, Alexandra | es |
dc.creator | Distaso, Monica | es |
dc.creator | Peukert, Wolfgang | es |
dc.creator | Schwieger, Wilhelm | es |
dc.creator | Spiecker, Erdmann | es |
dc.date.accessioned | 2018-12-07T11:58:11Z | |
dc.date.available | 2018-12-07T11:58:11Z | |
dc.date.issued | 2018 | |
dc.identifier.citation | Przybilla, T., Zubiri, B., Beltrán, A.M., Butz, B., Machoke, A.G., Inayat, A.,...,Spiecker, E. (2018). Transfer of Individual Micro- and Nanoparticles for High- Precision 3D Analysis Using 360° Electron Tomography. Small Methods, 2 (1), 1700276-. | |
dc.identifier.issn | 2366-9608 | es |
dc.identifier.uri | https://hdl.handle.net/11441/80850 | |
dc.description.abstract | A versatile approach is demonstrated, providing a general routine for
an extensive and advanced 3D characterization of individually selected
micro- and nanoparticles, enabling the combination of complementary and
scale-bridging techniques. Quintessential to the method is the transfer of
individual particles onto tailored tips using a conventional scanning electron
microscope equipped with a suitable micromanipulator. The method enables
a damage- and contamination-free preparation of freestanding particles. This
is of significant importance for applications addressing the measurement of
structural, physical, and chemical properties of specifically selected particles,
such as 360° electron tomography, atom probe tomography, nano X-ray
tomography, or optical near-field measurements. In this context, the method
is demonstrated for 360° electron tomography of micro-/macroporous zeolite
particles with sizes in the micrometer range and mesoporous alpha-hematite
nanoparticles exhibiting sizes of 50–100 nm, including detailed pre- and postcharacterization
on the nanoscale. | es |
dc.description.sponsorship | “Deutsche Forschungsgemeinschaft” (DFG) within the framework of the SPP 1570 (project DFG SP 648/4-3 “3D analysis of complex pore structures using ET and high-resolution TEM”) and the research training group GRK 1896 (“In situ Microscopy with Electrons, X-rays and Scanning Probes”) as well as through the Cluster of Excellence “Engineering of Advanced Materials” at the Friedrich-Alexander-Universität Erlangen-Nürnberg (Germany) | es |
dc.description.sponsorship | FIB | es |
dc.description.sponsorship | Julian Loscher | es |
dc.format | application/pdf | es |
dc.language.iso | eng | es |
dc.publisher | Wiley | es |
dc.relation.ispartof | Small Methods, 2 (1), 1700276-. | |
dc.rights | Attribution-NonCommercial-NoDerivatives 4.0 Internacional | * |
dc.rights.uri | http://creativecommons.org/licenses/by-nc-nd/4.0/ | * |
dc.subject | 360° electron tomography | es |
dc.subject | Dual-beam SEM/FIB | es |
dc.subject | Micromanipulation | es |
dc.subject | Pick and place | es |
dc.subject | Sample preparation | es |
dc.title | Transfer of Individual Micro- and Nanoparticles for High- Precision 3D Analysis Using 360° Electron Tomography | es |
dc.type | info:eu-repo/semantics/article | es |
dcterms.identifier | https://ror.org/03yxnpp24 | |
dc.type.version | info:eu-repo/semantics/publishedVersion | es |
dc.rights.accessRights | info:eu-repo/semantics/openAccess | es |
dc.contributor.affiliation | Universidad de Sevilla. Departamento de Ingeniería y Ciencia de los Materiales y del Transporte | es |
dc.relation.projectID | DFG SP 648/4-3 | es |
dc.relation.publisherversion | https://onlinelibrary.wiley.com/doi/full/10.1002/smtd.201700276 | es |
dc.identifier.doi | 10.1002/smtd.201700276 | es |
dc.contributor.group | Universidad de Sevilla. TEP123: Metalurgia e Ingeniería de los Materiales | es |
idus.format.extent | 7 p. | es |
dc.journaltitle | Small Methods | es |
dc.publication.volumen | 2 | es |
dc.publication.issue | 1 | es |
dc.publication.initialPage | 1700276 | es |
dc.contributor.funder | Deutsche Forschungsgemeinschaft / German Research Foundation (DFG) | |