Article
Applications of sample-controlled thermal analysis (SCTA) to kinetic analysis and synthesis of materials
Author/s | Pérez Maqueda, Luis Allan
Criado Luque, José Manuel Sánchez Jiménez, Pedro Enrique Diánez Millán, María Jesús |
Department | Universidad de Sevilla. Departamento de Química Inorgánica |
Publication Date | 2015 |
Deposit Date | 2018-04-10 |
Published in |
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Abstract | The advantages of the sample-controlled thermal analysis (SCTA) for both the kinetic analysis of solid-state reactions and the synthesis of materials are reviewed. This method implies an intelligent control of the temperature ... The advantages of the sample-controlled thermal analysis (SCTA) for both the kinetic analysis of solid-state reactions and the synthesis of materials are reviewed. This method implies an intelligent control of the temperature by the solid-state reaction under study in such a way that the reaction rate as a function of the time fits a profile previously defined by the user. It has been shown that SCTA has important advantages for discriminating the kinetic model of solid-state reactions as compared with conventional rising temperature methods. Moreover, the advantages of SCTA methods for synthesising materials with controlled texture and structure are analysed. |
Citation | Pérez Maqueda, L.A., Criado Luque, J.M., Sánchez Jiménez, P.E. y Diánez Millán, M.J. (2015). Applications of sample-controlled thermal analysis (SCTA) to kinetic analysis and synthesis of materials. Journal of Thermal Analysis and Calorimetry, 120, 45-51. |
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