Article
Structure of 5-fl-D-Galactopyranosyl- 1,3-dimethylbarbituric Acid Monohydrate,* C12H1sN2Os.H20
Author/s | Millán, M.
Conde Amiano, Clara Francisca Conde Amiano, Alejandro Márquez Delgado, Rafael |
Department | Universidad de Sevilla. Departamento de Física de la Materia Condensada |
Publication Date | 1985 |
Deposit Date | 2017-12-13 |
Published in |
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Abstract | Mr=336'30, orthorhombic, P21212 ~, a=
9.147(1), b=23.054(2), c=6.921(1)A, V=
1459.5(3)A 3, Z=4, Dm=l'53(1), Dx=
1.531Mgm -3, MoKa, 2=0.7107A, #=0.12mm -1,
F(000)= 712, T= 300K, R =0.055 for 1623 observed
independent ... Mr=336'30, orthorhombic, P21212 ~, a= 9.147(1), b=23.054(2), c=6.921(1)A, V= 1459.5(3)A 3, Z=4, Dm=l'53(1), Dx= 1.531Mgm -3, MoKa, 2=0.7107A, #=0.12mm -1, F(000)= 712, T= 300K, R =0.055 for 1623 observed independent reflexions. The galactopyranose ring adopts a 4C l conformation and the dihedral angle between the two rings in the molecule is 89.1 (1) °. The molecules are linked by an extensive three-dimensional hydrogen-bond network involving the water hydration molecule which stabilizes the crystal structure. |
Citation | Millán, M., Conde Amiano, C.F., Conde Amiano, A. y Márquez, R. (1985). Structure of 5-fl-D-Galactopyranosyl- 1,3-dimethylbarbituric Acid Monohydrate,* C12H1sN2Os.H20. Acta crystallographica. Section C, Crystal structure communications, 41 (FEB), 274-277. |
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