dc.creator | Barreales Suárez, Sofía | es |
dc.creator | Callejón Mochón, Manuel | es |
dc.creator | Azoulay, Stéphane | es |
dc.creator | Bello López, Miguel Ángel | es |
dc.creator | Fernández Torres, Rut | es |
dc.date.accessioned | 2024-01-11T14:18:21Z | |
dc.date.available | 2024-01-11T14:18:21Z | |
dc.date.issued | 2018 | |
dc.identifier.citation | Barreales Suárez, S., Callejón Mochón, M., Azoulay, S., Bello López, M.Á. y Fernández Torres, R. (2018). Liquid Chromatography Quadrupole Time-of-flight Mass Spectrometry Determination of Six Pharmaceuticals in Vegetal Biota. Uptake Study in Lavandula Dentata. Science of the Total Environment, 622-623, 655-663. https://doi.org/10.1016/j.scitotenv.2017.11.244. | |
dc.identifier.issn | 0048-9697 | es |
dc.identifier.issn | 1879-1026 | es |
dc.identifier.uri | https://hdl.handle.net/11441/153250 | |
dc.description.abstract | A procedure based on microwave assisted extraction for the determination of 6 pharmaceuticals in samples of Lavandula dentata, Salicornia ramosissima and Juncus sp. by liquid chromatography-quadrupole time of flight mass spectrometry (LC-QTOF/MS) was optimized and validated. Best results were obtained using microwave assisted extraction of 1.0 g of homogeneous lyophilized samples and 5 mL of a mixture ACN:H2O (1:1 v/v) as extracting solvent. Analytical recoveries ranged from 60 to 107% with relative standard deviation (RSD) lower than 15%. Limits of quantitation (LOQ) for the 6 pharmaceuticals flumequine (FLM), carbamazepine (CBZ), ciprofloxacin (CPR), enrofloxacin (ENR), diclofenac (DCL), and ibuprofen (IBU) were in the range 20.8–125 ng g− 1. The method was satisfactory applied for an uptake study in Lavandula dentata samples finding quantifying concentrations of FLM and CBZ in roots, leaf and stem. | es |
dc.description.sponsorship | Ministerio de Educación, Cultura y Deporte CTM2015-67902-C-1-P | es |
dc.description.sponsorship | European Commission. Fondo Europeo de Desarrollo Regional UNSE10-1E-429 | es |
dc.format | application/pdf | es |
dc.format.extent | 26 p. | es |
dc.language.iso | eng | es |
dc.publisher | Elsevier | es |
dc.relation.ispartof | Science of the Total Environment, 622-623, 655-663. | |
dc.rights | Attribution-NonCommercial-NoDerivatives 4.0 Internacional | * |
dc.rights.uri | http://creativecommons.org/licenses/by-nc-nd/4.0/ | * |
dc.subject | Juncus | es |
dc.subject | Lavandula dentata | es |
dc.subject | Liquid chromatography quadrupole time-of-flight | es |
dc.subject | Microwave extraction | es |
dc.subject | Pharmaceuticals | es |
dc.subject | Salicornia | es |
dc.title | Liquid Chromatography Quadrupole Time-of-flight Mass Spectrometry Determination of Six Pharmaceuticals in Vegetal Biota. Uptake Study in Lavandula Dentata | es |
dc.type | info:eu-repo/semantics/article | es |
dcterms.identifier | https://ror.org/03yxnpp24 | |
dc.type.version | info:eu-repo/semantics/acceptedVersion | es |
dc.rights.accessRights | info:eu-repo/semantics/openAccess | es |
dc.contributor.affiliation | Universidad de Sevilla. Departamento de Química Analítica | es |
dc.relation.projectID | CTM2015-67902-C-1-P | es |
dc.relation.projectID | UNSE10-1E-429 | es |
dc.relation.publisherversion | https://doi.org/10.1016/j.scitotenv.2017.11.244 | es |
dc.identifier.doi | 10.1016/j.scitotenv.2017.11.244 | es |
dc.journaltitle | Science of the Total Environment | es |
dc.publication.volumen | 622-623 | es |
dc.publication.initialPage | 655 | es |
dc.publication.endPage | 663 | es |
dc.contributor.funder | Ministerio de Educación, Cultura y Deporte (MECD). España | es |
dc.contributor.funder | European Commission (EC). Fondo Europeo de Desarrollo Regional (FEDER) | es |