dc.creator | Salvo, Christopher | es |
dc.creator | Chicardi Augusto, Ernesto | es |
dc.creator | Poyato, Rosalía | es |
dc.creator | García-Garrido, Cristina | es |
dc.creator | Jiménez, José Antonio | es |
dc.creator | López Pernía, Cristina | es |
dc.creator | Tobosque, Pablo | es |
dc.creator | Mangalaraja, Ramalinga Viswanathan | es |
dc.date.accessioned | 2021-06-21T16:25:14Z | |
dc.date.available | 2021-06-21T16:25:14Z | |
dc.date.issued | 2021 | |
dc.identifier.citation | Salvo, C., Chicardi Augusto, E., Poyato, R., García-Garrido, C., Jiménez, J.A., López Pernía, C.,..., Mangalaraja, R. V. (2021). Synthesis and Characterization of a Nearly Single Bulk Ti2AlN MAX Phase Obtained from Ti/AlN Powder Mixture through Spark Plasma Sintering. Materials, 14 (9), Article number 2217. | |
dc.identifier.issn | 1996-1944 | es |
dc.identifier.uri | https://hdl.handle.net/11441/114705 | |
dc.description | Article number 2217 | es |
dc.description.abstract | MAX phases are an advanced class of ceramics based on ternary carbides or nitrides that
combine some of the ceramic and metallic properties, which make them potential candidate materials
for many engineering applications under severe conditions. The present work reports the successful
synthesis of nearly single bulk Ti2AlN MAX phase (>98% purity) through solid-state reaction and
from a Ti and AlN powder mixture in a molar ratio of 2:1 as starting materials. The mixture of Ti
and AlN powders was subjected to reactive spark plasma sintering (SPS) under 30 MPa at 1200 ◦C
and 1300 ◦C for 10 min in a vacuum atmosphere. It was found that the massive formation of Al2O3
particles at the grain boundaries during sintering inhibits the development of the Ti2AlN MAX phase
in the outer zone of the samples. The effect of sintering temperature on the microstructure and
mechanical properties of the Ti2AlN MAX phase was investigated and discussed. | es |
dc.description.sponsorship | Agencia Nacional de Investigación y Desarrollo de la Gobierno de Chile (ANID)11200924 | es |
dc.format | application/pdf | es |
dc.format.extent | 11 p. | es |
dc.language.iso | eng | es |
dc.publisher | MDPI | es |
dc.relation.ispartof | Materials, 14 (9), Article number 2217. | |
dc.rights | Attribution-NonCommercial-NoDerivatives 4.0 Internacional | * |
dc.rights.uri | http://creativecommons.org/licenses/by-nc-nd/4.0/ | * |
dc.subject | MAX phase | es |
dc.subject | Ti2AlN | es |
dc.subject | Spark plasma sintering | es |
dc.title | Synthesis and Characterization of a Nearly Single Bulk Ti2AlN MAX Phase Obtained from Ti/AlN Powder Mixture through Spark Plasma Sintering | es |
dc.type | info:eu-repo/semantics/article | es |
dcterms.identifier | https://ror.org/03yxnpp24 | |
dc.type.version | info:eu-repo/semantics/publishedVersion | es |
dc.rights.accessRights | info:eu-repo/semantics/openAccess | es |
dc.contributor.affiliation | Universidad de Sevilla. Departamento de Ingeniería y Ciencia de los Materiales y del Transporte | es |
dc.contributor.affiliation | Universidad de Sevilla. Departamento de Física de la Materia Condensada | es |
dc.relation.projectID | 11200924 | es |
dc.relation.publisherversion | https://www.mdpi.com/1996-1944/14/9/2217 | es |
dc.identifier.doi | 10.3390/ma14092217 | es |
dc.journaltitle | Materials | es |
dc.publication.volumen | 14 | es |
dc.publication.issue | 9 | es |
dc.publication.initialPage | Article number 2217 | es |