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Applications of sample-controlled thermal analysis (SCTA) to kinetic analysis and synthesis of materials

 

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Opened Access Applications of sample-controlled thermal analysis (SCTA) to kinetic analysis and synthesis of materials
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Author: Pérez Maqueda, Luis Allan
Criado Luque, José Manuel
Sánchez Jiménez, Pedro Enrique
Diánez Millán, María Jesús
Department: Universidad de Sevilla. Departamento de Química Inorgánica
Date: 2015
Published in: Journal of Thermal Analysis and Calorimetry, 120, 45-51.
Document type: Article
Abstract: The advantages of the sample-controlled thermal analysis (SCTA) for both the kinetic analysis of solid-state reactions and the synthesis of materials are reviewed. This method implies an intelligent control of the temperature by the solid-state reaction under study in such a way that the reaction rate as a function of the time fits a profile previously defined by the user. It has been shown that SCTA has important advantages for discriminating the kinetic model of solid-state reactions as compared with conventional rising temperature methods. Moreover, the advantages of SCTA methods for synthesising materials with controlled texture and structure are analysed.
Cite: Pérez Maqueda, L.A., Criado Luque, J.M., Sánchez Jiménez, P.E. y Diánez Millán, M.J. (2015). Applications of sample-controlled thermal analysis (SCTA) to kinetic analysis and synthesis of materials. Journal of Thermal Analysis and Calorimetry, 120, 45-51.
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URI: https://hdl.handle.net/11441/72291

DOI: 10.1007/s10973-014-4176-6

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