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Structure and Absolute Configuration of l'-(p-Bromophenyl)-3'-ethyl-l',Y,4',5'- tetrahydro- 1,2-dideoxy-u-L-glucofuranoso[2,l-d]imidazole-2'-thione Monohydrate,* C15H19BrN204S.H20

 

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Opened Access Structure and Absolute Configuration of l'-(p-Bromophenyl)-3'-ethyl-l',Y,4',5'- tetrahydro- 1,2-dideoxy-u-L-glucofuranoso[2,l-d]imidazole-2'-thione Monohydrate,* C15H19BrN204S.H20
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Author: Conde Amiano, Clara Francisca
Millán, M.
Conde Amiano, Alejandro
Márquez Delgado, Rafael
Department: Universidad de Sevilla. Departamento de Física de la Materia Condensada
Date: 1985
Published in: Acta crystallographica. Section C, Crystal structure communications, 41 (FEB), 277-280.
Document type: Article
Abstract: M r = 421-30, monoclinic, P2~, a = 7.531 (1), b=8.148(4), c= 14. 625 (2) ,~, fl=97.14(1) °, V= 890.5 (5) ,~3, Z= 2, Din= 1.58 (1), Dx= 1.571 Mg m -3, Mo Kct, 2 = 0.7107 ,~,/~ = 2.42 mm -1, F(000)=432, T= 300 K, R =0.065 for 1672 observed independent reflexions. The sugar ring adopts a 4T 3 conformation and the dihedral angle in the bicyclic system is 72.3 (4) °. A three-dimensional network of hydrogen bonds links the molecules to build up the crystal structure.
Cite: Conde Amiano, C.F., Millán, M., Conde Amiano, A. y Márquez, R. (1985). Structure and Absolute Configuration of l'-(p-Bromophenyl)-3'-ethyl-l',Y,4',5'- tetrahydro- 1,2-dideoxy-u-L-glucofuranoso[2,l-d]imidazole-2'-thione Monohydrate,* C15H19BrN204S.H20. Acta crystallographica. Section C, Crystal structure communications, 41 (FEB), 277-280.
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URI: http://hdl.handle.net/11441/67623

DOI: 10.1107/S0108270185003614

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