Artículo
Synthesis and tribological properties of WSex films prepared by magnetron sputtering
Autor/es | Domínguez Meister, Santiago
Justo Erbez, Ángel J. Sánchez López, Juan Carlos |
Fecha de publicación | 2013 |
Fecha de depósito | 2018-12-05 |
Publicado en |
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Resumen | WSex films with variable Se/W ratio were deposited by non-reactive r.f. magnetron sputtering from WSe2 target changing the applied d.c. pulsed bias conditions and substrate temperature. The structural and chemical properties ... WSex films with variable Se/W ratio were deposited by non-reactive r.f. magnetron sputtering from WSe2 target changing the applied d.c. pulsed bias conditions and substrate temperature. The structural and chemical properties were measured by cross-sectional scanning electron microscopy (X-SEM), energy dispersive analysis (EDX), X-ray diffraction (XRD), Raman and X-ray photoelectron spectroscopy (XPS). The tribological properties were measured in ambient air (RH = 30–40%) and dry nitrogen by means of a reciprocating ball-on-disk tribometer. A clear correlation was found between the Se/W ratio and the measured friction coefficient displaying values below 0.1 (in ambient air) and 0.03 (in dry N2) for ratios Se/W ≥ 0.6 as determined by electron probe microanalysis (EPMA). The results demonstrated that notable tribological results could be obtained even in ambient air (friction ≤ 0.07 and wear rate ≈10−7 mm3 Nm−1) by controlling the film microstructure and chemical composition. By incorporating carbon, wear and chemical resistance can be gained by formation of non-stoichiometric carbides and/or alloying into the defective WSex hexagonal structure. The existence of a WSe2 rich interfacial layer (either on the ball scar or embedded in the film track) was evidenced by Raman in low friction conditions. The improvement in tribological performance is therefore obtained by means of layered WSex, the formation of gradient composition from metallic W (hard) to WSe2 (lubricant) and carbon incorporation. |
Agencias financiadoras | Ministerio de Educación y Ciencia (MEC). España Junta de Andalucía |
Identificador del proyecto | MAT2010-21597-C02-01
MAT2011-29074-C02-01 CSD2008-00023 P10-TEP- 67182 |
Cita | Domínguez Meister, S., Justo Erbez, Á.J. y Sánchez López, J.C. (2013). Synthesis and tribological properties of WSex films prepared by magnetron sputtering. Materials Chemistry and Physics, 142 (1), 186-194. |
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