dc.creator | Rivero Antúnez, Pedro | es |
dc.creator | Cano Crespo, Rafael | es |
dc.creator | Sánchez Bajo, Florentino | es |
dc.creator | Domínguez Rodríguez, Arturo | es |
dc.creator | Morales Flórez, Víctor | es |
dc.date.accessioned | 2022-10-19T16:06:40Z | |
dc.date.available | 2022-10-19T16:06:40Z | |
dc.date.issued | 2021 | |
dc.identifier.citation | Rivero Antúnez, P., Cano Crespo, R., Sánchez Bajo, F., Domínguez Rodríguez, A. y Morales Flórez, V. (2021). Reactive SPS for sol–gel alumina samples: Structure, sintering behavior, and mechanical properties. Journal of the European Ceramic Society, 41 (11), 5548-5547. https://doi.org/10.1016/j.jeurceramsoc.2021.04.060. | |
dc.identifier.issn | 0955-2219 | es |
dc.identifier.issn | 1873-619X | es |
dc.identifier.uri | https://hdl.handle.net/11441/138143 | |
dc.description.abstract | This work presents a fast and direct controlled routine for the fabrication of fully dense alumina based on the reactive spark plasma sintering (reactive-SPS) of boehmite (γ-AlOOH) nano-powders obtained by the sol–gel technique. The evolution of the transition aluminas during sintering has been studied. Some boehmite powders were seeded with α-Al2O3 particles prior to the gelation. Boehmite seeded powders exhibited a direct transition to α-Al2O3 at 1070 °C, enhancing the transformation kinetics and lowering the required temperature by more than 100 °C. For comparison, other samples were prepared by previously annealing the seeded and unseeded boehmite powders. Thus, α-Al2O3 powders were obtained and were sintered by standard-SPS. A detailed structural and mechanical characterization is presented, comparing the hardness and indentation fracture resistance for different grain sizes and porosities. Both the reactive-SPSed samples and the standard-SPSed samples showed a high hardness (18–20 GPa), whereas the reactive-SPSed samples exhibited a lower indentation fracture resistance due to a large grain size (∼10 μm). Improvements of this procedure for obtaining smaller grain size are discussed. In summary, the presented technique brings a revolutionary fast method for the fabrication of fully dense alumina, as this process reduces the time and temperature required for alumina densification. | es |
dc.description.sponsorship | Ministerio de Ciencia e Innovación PGC2018-094952-B-I00 | es |
dc.description.sponsorship | Junta de Andalucía P12- FQM-1079, FQM393 | es |
dc.description.sponsorship | Universidad de Sevilla PGC2018-094952-B-I00 | es |
dc.description.sponsorship | Junta de Extremadura GR18081 | es |
dc.format | application/pdf | es |
dc.format.extent | 10 p. | es |
dc.language.iso | eng | es |
dc.publisher | Elsevier | es |
dc.relation.ispartof | Journal of the European Ceramic Society, 41 (11), 5548-5547. | |
dc.rights | Attribution-NonCommercial-NoDerivatives 4.0 Internacional | * |
dc.rights.uri | http://creativecommons.org/licenses/by-nc-nd/4.0/ | * |
dc.subject | Boehmite | es |
dc.subject | Fracture toughness | es |
dc.subject | Reactive SPS sintering | es |
dc.subject | Vickers hardness | es |
dc.subject | α-Al2O3 | es |
dc.title | Reactive SPS for sol–gel alumina samples: Structure, sintering behavior, and mechanical properties | es |
dc.type | info:eu-repo/semantics/article | es |
dcterms.identifier | https://ror.org/03yxnpp24 | |
dc.type.version | info:eu-repo/semantics/publishedVersion | es |
dc.rights.accessRights | info:eu-repo/semantics/openAccess | es |
dc.contributor.affiliation | Universidad de Sevilla. Departamento de Física de la Materia Condensada | es |
dc.relation.projectID | PGC2018-094952-B-I00 | es |
dc.relation.projectID | P12- FQM-1079 | es |
dc.relation.projectID | FQM393 | es |
dc.relation.projectID | PGC2018-094952-B-I00 | es |
dc.relation.projectID | GR18081 | es |
dc.relation.publisherversion | https://doi.org/10.1016/j.jeurceramsoc.2021.04.060 | es |
dc.identifier.doi | 10.1016/j.jeurceramsoc.2021.04.060 | es |
dc.journaltitle | Journal of the European Ceramic Society | es |
dc.publication.volumen | 41 | es |
dc.publication.issue | 11 | es |
dc.publication.initialPage | 5548 | es |
dc.publication.endPage | 5547 | es |
dc.contributor.funder | Ministerio de Ciencia e Innovación (MICIN). España | es |
dc.contributor.funder | Junta de Andalucía | es |
dc.contributor.funder | Universidad de Sevilla | es |
dc.contributor.funder | Junta de Extremadura | es |
dc.description.awardwinning | Premio Mensual Publicación Científica Destacada de la US. Facultad de Física | |