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Artículo
Large-scale preparation and labelling reactions of deuterated silanes
(John Wiley & Sons, 2012)
A catalytic synthesis of deuterated silanes SiEt3D, SiMe2PhD and SiPh2D2 is reported that allows their facile generation in a 3–4 g scale, utilizing D2 (0.5 bar) as the hydrogen isotope source and low catalyst loadings ...