Ipus Bados, Jhon JairoBlázquez Gámez, Javier SebastiánLozano Pérez, SergioConde Amiano, Alejandro2023-06-122023-06-122009Ipus Bados, J.J., Blázquez Gámez, J.S., Lozano Pérez, S. y Conde Amiano, A. (2009). Microstructural Evolution Characterization of Fe-Nb-B Ternary Systems Processed by Ball Milling. Philosophical Magazine, 89 (17), 1415-1423. https://doi.org/10.1080/14786430902984566.1478-64351478-6443https://hdl.handle.net/11441/147087Fe-Nb-B alloys prepared by ball milling can undergo a complex microstructural evolution during milling. In order to overcome the limitations imposed by traditional X-ray bulk analysis, a comprehensive multi-technique approach was devised to systematically characterize samples with the required resolution. A combination of in situ FIB (focused ion beam) lift-out and high-resolution ATEM (analytical transmission electron microscopy) has allowed the characterization of the phase evolution during milling. In particular, boron inclusions, not detected by X-ray diffraction, have been found to remain undissolved in the Fe matrix.application/pdf18 p.engAtribución-NoComercial 4.0 Internacionalhttp://creativecommons.org/licenses/by-nc/4.0/Amorphous alloyBall millingFIBNanocrystalline alloyTEMinfo:eu-repo/semantics/articleinfo:eu-repo/semantics/openAccesshttps://doi.org/10.1080/14786430902984566