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Now showing items 1-8 of 8
Article
Influence of the milling parameters on the mechanical work intensity in planetary mills
(Elsevier, 2013)
The formation of ZnSe via a mechanically-induced self-sustaining reaction (MSR) from a Zn/Se mixture showed that only size reduction and mixing of the reactants without product formation occurred during the induction period ...
Article
Room temperature mechanosynthesis of the La 1-xSr xMnO 3±δ (0≤x≤1) system and microstructural study
(Elsevier, 2012)
Monophase nanocrystalline powders belonging to the La 1-xSr xMnO 3±δ system (0≤x≤1) with a perovskite structure have been obtained by mechanochemistry synthesis using a planetary ball milling equipment from La 2O 3, SrO, ...
Article
Chalcogenide Quaternary Cu2FeSnS4 Nanocrystals for Solar Cells: Explosive Character of Mechanochemical Synthesis and Environmental Challenge
(MDPI, 2017)
In this study we demonstrate the synthesis of quaternary semiconductor nanocrystals of stannite Cu2FeSnS4/rhodostannite Cu2FeSn3S8 (CFTS) via mechanochemical route using Cu, Fe, Sn and S elements as precursors in one-pot ...
Article
Synthesis of Mn2+-doped ZnS by a Mechanically Induced Self-sustaining Reaction
(Springer Nature, 2020)
The mechanochemical process denoted as a mechanically induced self-sustaining reaction was successfully applied in obtaining Mn-doped ZnS samples with Mn content between 0 and 5 mol%. The process consists in milling Zn/Mn/S ...
Article
Inverse core-rim microstructure in (Ti,Ta)(C,N)-based cermets developed by a mechanically induced self-sustaining reaction
(Elsevier, 2012)
Cermets with a nominal composition (Ti 0.8Ta 0.2C 0.5N 0.5- 20 wt.% Co) were synthesised by a mechanically induced self-sustaining reaction (MSR) process from stoichiometric elemental powder blends. The MSR allowed the ...
Article
TiTaCN-Co cermets prepared by mechanochemical technique: microstructure and mechanical properties
(Elsevier, 2016)
Microstructure and mechanical characterization of (Ti,Ta)(C,N)-Co based solid solution cermets prepared by two mechanochemical synthesis processes (one- and two-step milling) and a pressureless sintering in protective ...
Article
Mechanochemical Solvent-Free Synthesis of Quaternary Semiconductor Cu-Fe-Sn-S Nanocrystals
(SpringerOpen, 2017)
In this study, we demonstrate a one-pot mechanochemical synthesis of the nanocomposite composed of stannite Cu2FeSnS4 and rhodostannite Cu2FeSn3S8 nanocrystals using a planetary ball mill and elemental precursors (Cu, Fe, ...
Article
Chemical and electrical properties of LSM cathodes prepared by mechanosynthesis
(Elsevier, 2014)
Mechanosynthesis of La1-xSrxMnO3 (x = 0, 0.25, 0.5, 0.75 and 1) was carried out at room temperature from stoichiometric mixtures of La2O3, Mn2O3 and SrO, obtaining monophasic powders with the perovskite structure. Physical ...